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분야
pptx2.Experimental
Synthesis of MA
PEI impregnation on MA
Amine grafting on MCM-41
Characterization of the materials prepared
CO2 adsorption-desorption measurement
3.Results and discussion
Physical properties of MA
CO2 adsorption by MA
CO2 sorption by PEI-impregnated MA
4.Conclusion
5.Reference
A large amount of amine-type CO2 capturing agent into its mesopores in a well dispersed manner
Synthesis of MA
PEI impregnation on MA
Amine grafting on MCM-41
Characterization of the materials prepared
CO2 adsorption-desorption measurement
Al(i-PrO)3 (41.68g)+ Alcohol solvent
(EtOH 73.6g + isopropanol 72.2g) at 50oC
Distilled water (7.2g) – promote hydrolysis
Stirring – 9 hr at room temp
Heat (sol)- 70oC for 24 hr in oven
Heat (gel)- 120oC for 12 hr in autoclave
Washing with EtOH and drying
The Barrett-Joyner-Halenda (BJH) method for calculating pore size distributions is based on a model of the adsorbent as a collection of cylindrical pores. The theory accounts for capillary condensation in the pores using the classical Kelvin equation, which in turn assumes a hemispherical liquid-vapor meniscus and a well-defined surface tension.
CO2 capture using mesoporous alumina prepared by a sol–gel process
http://blog.naver.com/bluesagua?Redirect=Log&logNo=110035377651
Development of high stability catalysts to facilitate CO2 capture into water - an alternative to monoethanolamine and amine solvents
Designing small-molecule catalysts for CO2 capture
http://tdworld.com/business/alstom-ccs-project-results-0511
http://ec.europa.eu/research/energy/pdf/synopses_co2_en.pdf
http://amigas.kaist.ac.kr/zbxe/r_board/213
