B. Solution-Liquid-Solid Growth of Indium Phosphide Fibers from Organometallic Precursors: Elucidation of Molecular and Nonmolecular Components of the Pathway
Solution-phase organometallic syntheses of semiconductors are used for the growth of high-quality quantum dots,1-3 and are potentially useful for the deposition of semiconductor materials on thermally sensitive substrates such as polymers
3. Experiment
재료의 강도와 경도에 영향을 미치는 변수는 다양함.
재료의 밀도가 영향을 크게 미치긴 하지만 그 외에도 상의 형성 방법이나 소결 조건에 따라서도 달라짐.
그래서 재료의 강도 및 경도를 예측할 척도로 밀도를 측정하고자 함
상대밀도로 이론적인 밀도와 상대밀도를 비교하여
Sol-Gel법
Sol: 액상에 고체입자가 분산되어 있는 콜로이드
- Aerosol : 기상에 고체입자 혹은 액적이 분산
- Emulsion : 액상에 액적이 분산
Gel: Sol의 입자들이 물리적인 힘으로 연결되어
형성(gelation)된 망상조직.
- Xerogel : 상압에서 Sol용액을 증발시켜 얻은 젤
- Aerogel : 고온 감압 하에서
2. Experimental
The films were deposited in a conventional horizontal furnace on Si(1 1 1) substrates. SnO2 (99.99%) (Mol10:2) and ZnO/Ge slices (99.999%, purity), (Mol 10:2) powders were used as the source materials for growth of the Sn- and Ge-doped ZnO films, respectively. The ZnO/SnO2 powder was placed on an alumina boat and inserted into a horizontal tube furnace, in order to serve as th
powders were mixed at a molar ratio of 10:1 @ 40 Mpa
The pill was calcined in a box furnace @ 500 C for 5 h and sintered @900 C for 12 h in the air
1. The powder was placed on an alumina boat and inserted into a horizontal tube furnace
2. Silicon substrates were located downstream from the source material @ 700 and 800 C.
3. A vacuum of 6 Torr was maintained inside the furnace tube during