The reaction occurs just with 1/20~1/60 of HCl
requirements in the reaction formula.
3-neck flask
The flasks are often long neck; sometimes they have the incision on the neck, which precisely defines the volume of flask.
They can be used in distillations, or in the heating a product.
These types of flask are alternatively called Florence flasks.
Liebig condenser
the most ba
Synthesize aniline by the reduction with iron and hydrochloric acid
Amination
Process by which an amine group is introduced into an organic molecule
- Ammonolysis : reaction with ammonia or another amine such as an alkylation
Ex)RX+NHv → RNHv+HX
RCOCl+2NH3 → RCONH2+NH4Cl
RCOOC2H5+NH3 → RCONH2+C2H5OH
- Reduction : reductive amination with m
1. 실험 제목
Aniline synthesis
2. 실험목적
주석과 염산을 이용하여 니트로벤젠으로부터 아닐린을 제조하여 보고, 여러가지 유기화합물의 반응 중 하나인 아미노화 반응의 원리를 이해한다.
3. 실험이론
1) 아닐린 (Aniline)
화학식은 C6H7N으로 나이트로벤젠을 금속과 염산으로 환원시켜 만든 방향족